Analytical Instruments - "Spectroscan MAKC" spectrometers

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#A07

 «SPECTROSCAN MAKC-GV»

WDX spectrometer

«Spectroscan MAKC-GV» desktop x-ray fluorescent crystal diffraction scanning spectrometer is the most universal and modern instrument of «Spectroscan MAKC» brand. It can analyse elements from 11Na to 92U. The range of analysed elements is expanded due to development of vacuum chamber with goniometer and  5 automatically changeable crystal-analysers. The samples are outside the vacuum chamber; therefore any type of samples (solid, liquid, powder) can be analysed.

No external cooling systems, no liquid nitrogen, no gas pumping is required. Automatic sample changer for 16 samples has also two cells with spinning, providing representative analysis of heterogeneous samples.

High aperture scheme together with 200W x-ray tube provides high intensities of analytical lines, therefore sensitivity and express analysis.

Simplicity and flexibility of operation due to a user-friendly interface. Complete computer control of measurements, easy processing (automatic or manual). Quantitative, qualitative and standardless analysis.

Analytical Parameters
Element range

from 11Na  to  92U

Sample type liquid, solid, powders, filters, films
Detection limits for light matrix (time 100 sec.) Na — 1´10-1 %, Mg, — 1´10-2 %, Al — 1´10-3 %,
Si — 5´10-4 %, P — 5´10-4 %, Cd, Pb — 5´10-4 %
S,
Ti, V, Cr — 1´10-4 %,Co, Ni — 5´10-5 %,
Concentration range
without sample preparation
with special sample preparation
from 3L to 100%
from  0,005 L
Line detection crystal diffraction
Quantitative analysis time for a sample from  3 minutes
Time of one element determination from 10 to 100 seconds
X-ray layout Johansson scheme
Energy resolution 9 eV (Si Ka) 60 eV ( Fe Ka)
Apparatus error 0,5 %

Technical parameters

Maximum X-ray tube voltage 50 êÂ
Crystal analyzers for Johan and Johansson schemes LiF(200), C, PET, KAP, ML (44E)
Sample changer

Automatic sample changer for 16 samples :

14 -  20mm diameter and  

2 samples 40 mm in diameter with spinning

Size and weight

spectrometric unit
High voltage source
Vacuum pump block

550´450´450 mm; 70 kg
240´440´450 mm; 30 kg
130´200´320 mm; 15 kg
Closed cycle water cooling  
Power supply
Consumed capacity from the mains 220 V
~220 Â, 50 Hz, ~ 380 V
850 W
PC interface RS-232

Applications

metallurgy, mining and chemistry

 

Raw material and end product analysis.

Ores and minerals analysis.

machine-building

 

Non-destructive examination of details and mechanisms. Alloys input control. Films and coating composition determination. Engineering diagnostics

gold mining, rare and precious metals processing

 

Materials composition analysis.

oil production, petroleum products processing and transportation

 

Chloride, sulfur, lead and heavy metals detection in petroleum and petroleum products. Petroleum and diesel fuel quality control.

ecological control

 

Water, soil and air pollution analysis.

agriculture, food processing

 

Microelements estimation in soils, food and livestock products. Heavy metals control in food.

art and forensic expertise

 

Non-destructive analysis of pieces of art, objects identification.